N-(2,6-Dimethyl­phen­yl)succinamic acid

نویسندگان

  • B. Thimme Gowda
  • Sabine Foro
  • B. S. Saraswathi
  • Hiromitsu Terao
  • Hartmut Fuess
چکیده

In the amide segment of the title compound, C(12)H(15)NO(3) {systematic name: 3-[(2,6-dimethyl-phen-yl)amino-carbon-yl]propionic acid}, the N-H and C=O bonds are anti to each other. The mol-ecules are packed into a two-dimensional array via N-H⋯O and O-H⋯O hydrogen bonds.

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منابع مشابه

N-(3,4-Dimethyl­phen­yl)succinamic acid

The asymmetric unit of the title compound, C(12)H(15)NO(3), contains two independent mol-ecules. In both mol-ecules, the conformations of the amide oxygen and the carbonyl O atom of the acid segment are anti to the adjacent CH(2) groups. In the crystal, both molecules form inversion dimers linked by pairs of O-H⋯O hydrogen bonds and N-H⋯O interactions link the dimers into [100] chains.

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N-(3,5-Dimethyl­phen­yl)succinamic acid

In the title compound, C(12)H(15)NO(3), the N-H and C=O bonds are anti to each other. The C=O and O-H bonds of the acid group display an anti-periplanar orientation relative to each other. The crystal packing features a three-dimensional network of molecules held together by O-H⋯O and N-H⋯O hydrogen bonds.

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N-(2,3-Dimethyl­phen­yl)succinamic acid

In the title compound, C(12)H(15)NO(3), the conformations of N-H and C=O bonds in the amide segment are anti to each other and that of the amide H atom is syn to the ortho- and meta-methyl groups in the benzene ring. In the crystal, the mol-ecules are linked into infinite chains through inter-molecular O-H⋯O and N-H⋯O hydrogen bonds.

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N 1,N 2-Bis­(2,6-di­methyl­phen­yl)-N 1-hydroxyformamidine N,N′-bis­(2,6-dimethyl­phen­yl)-N-oxidoformamidinium dichloro­methane solvate

The title compound, 2C(17)H(20)N(2)O·CH(2)Cl(2), was obtained by N-oxidation of the parent formamidine with m-chloro-peroxy-benzoic acid (m-CPBA). This is the first use of the above-mentioned synthetic route for the preparation of hydroxy-amidines. The title compound crystallizes as a cyclic dimer resulting from the presence of O-H⋯O and N-H⋯N hydrogen bonds.

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N-(2,6-Dimethyl­phen­yl)-2-methyl­acetamide

The structure of the title compound (26DMPMA), C(11)H(15)NO, is closely related to the side-chain unsubstituted N-(2,6-dimethyl-phen-yl)acetamide and side-chain substituted N-(2,6-dimethyl-phen-yl)-2,2,2-trimethyl-acetamide and 2-chloro-N-(2,6-dimethyl-phen-yl)acetamide, with slightly different bond parameters. The mol-ecules in 26DMPMA are linked into chains through N-H⋯O hydrogen bonding.

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عنوان ژورنال:

دوره 65  شماره 

صفحات  -

تاریخ انتشار 2009